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其他作者 | Radziemski, Leon J., 1937- |
版本 | 2nd ed |
說明 | 1 online resource |
附註 | Includes bibliographical references and index |
| Handbook of Laser-Induced Breakdown Spectroscopy; Contents; Preface; Acronyms, Constants, and Symbols; 1 Introduction; 1.1 Atomic Optical Emission Spectrochemistry (OES); 1.1.1 Conventional OES; 1.1.2 Laser OES; 1.2 Laser-Induced Breakdown Spectroscopy (LIBS); 1.3 LIBS History 1960-1980; 1.4 LIBS History 1981-1990; 1.5 LIBS History 1991-2000; 1.6 LIBS History 2001-2012; References; 2 Basics of the LIBS Plasma; 2.1 LIBS Plasma Fundamentals; 2.1.1 Spectral Lines and Line Profiles; 2.1.2 Determining Electron Densities from Spectral Line Widths; 2.1.3 Plasma Opacity |
| 2.1.4 Temperature and Thermodynamic Equilibrium2.2 Laser-Induced Breakdown; 2.2.1 Breakdown in Gases; 2.2.2 Post-Breakdown Phenomena in Gases; 2.2.3 Breakdown in and on Solids, Aerosols, and Liquids; 2.2.4 Post-Breakdown Phenomena on Solid Surfaces; 2.3 Laser Ablation from Surfaces and Aerosols; 2.4 Nanosecond and Femtosecond Double- or Multiple-Pulse LIBS; 2.5 Summary; 2.6 Problems; References; 3 LIBS Apparatus Fundamentals; 3.1 Basic LIBS Apparatus; 3.2 Lasers; 3.2.1 Laser Fundamentals; 3.2.2 Types of Lasers; 3.2.3 Properties of Laser Light Important for LIBS |
| 3.2.4 Generation of Additional Wavelengths3.2.5 Double-Pulse Operation; 3.3 Optical Systems; 3.3.1 Focusing and Light Collection; 3.3.2 Lenses; 3.3.3 Fiber Optic Cables; 3.4 Methods of Spectral Resolution; 3.4.1 Introduction; 3.4.2 Spectral Resolution Devices; 3.5 Detectors; 3.6 Detection System Calibrations; 3.6.1 Wavelength Calibration; 3.6.2 Spectral Response Calibration; 3.7 Timing Considerations; 3.8 Methods of LIBS Deployment; 3.9 Problems; References; 4 LIBS Analytical Figures of Merit and Calibration; 4.1 Introduction; 4.2 Basics of a LIBS Measurement; 4.3 Precision; 4.4 Calibration |
| 4.4.1 Calibration Curves4.4.2 Calibration Standards; 4.4.3 Calibration-Free LIBS; 4.5 Detection Limit; 4.6 Accuracy; 4.7 Problems; References; References for Detection Limits; 5 Qualitative LIBS Analysis; 5.1 Introduction; 5.2 Identifying Elements; 5.3 Material Identification; 5.4 Process Monitoring; 5.4.1 Introduction; 5.4.2 Experimental; 5.4.3 Results; 5.4.4 Conclusions; 5.5 Material Sorting/Distinguishing; 5.5.1 Surface Condition; 5.5.2 Type of Analysis; 5.5.3 Sorting Materials of Close Composition; 5.5.4 Other Examples of Material Identification; 5.6 Site Screening Using LIBS |
| 5.7 Semiquantitative Analysis5.8 Problems; References; 6 Quantitative LIBS Analysis; 6.1 Introduction; 6.2 Effects of Sampling Geometry; 6.3 Other Sampling Considerations; 6.4 Incomplete Vaporization and Ablation Stoichiometry; 6.5 Use of Internal Standardization; 6.6 Chemical Matrix Effects; 6.7 Example of LIBS Measurement: Impurities in Lithium-Containing Solutions; 6.7.1 Objective; 6.7.2 Experimental; 6.7.3 Results; 6.7.4 Discussion of Results; 6.8 Example of LIBS Measurement: Detection of Materials on Swipes; 6.8.1 Objective; 6.8.2 Experimental; 6.8.3 Results |
| "Starting from fundamentals and moving through a thorough discussion of equipment, methods, and techniques, the Handbook of Laser-Induced Breakdown Spectroscopy provides a unique reference source that will be of value for many years to come for this important new analysis method. The authors, with a total of over 60 years of experience in the LIBS method, use a combination of tutorial discussions ranging from basic principles up to more advanced descriptions along with extensive figures and photographs to clearly explain topics addressed in the text. In this second edition, chapters on the use of statistical analysis and advances in detection of weapons of mass destruction have been added. Tables of data related to analysis with LIBS have been updated. The Handbook of Laser-Induced Breakdown Spectroscopy, Second Edition: provides a thorough but understandable discussion of the basic principles of the method based on atomic emission spectroscopy, including recently available data leading to better characterization of the LIBS plasma; presents a discussion of the many advantages of the method along with limitations, to provide the reader a balanced overview of capabilities of the method; describes LIBS instrumentation ranging from basic set-ups to more advanced configurations; presents a comprehensive discussion of the different types of components (laser, spectrometers, detectors) that can be used for LIBS apparatuses along with suggestions for their use, as well as an up-to-date treatment of the newest advances and capabilities of LIBS instruments; presents the analytical capabilities of the method in terms of detection limits, accuracy, and precision of measurements for a variety of different sample types; discusses methods of sampling different media such as gases, liquids, and solids; presents an overview of some real-world applications of the method, with new emphasis on sampling of biologically and physically dangerous materials; provides an up-to-date list |
| "The only manual that goes from the simplest to the most complex and state-of-the-art embodiments of LIBS experimental set up"--Provided by publisher |
| Description based on print version record |
主題 | Atomic emission spectroscopy |
| Laser-induced breakdown spectroscopy |
ISBN/ISSN | 9781118567371 (electronic bk.) |
| 1118567374 (electronic bk.) |
| 9781118567340 (electronic bk.) |
| 111856734X (electronic bk.) |
| 9781118567357 |
| 1118567358 |
| 9781118567364 |
| 1118567366 |
| 9781119971122 (hardback) |
| 1119971128 (hardback) |